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The Analytical Chemistry of Silicones (Chemical Analysis: A Series of Monographs on Analytical Chemistry and Its Applications)
 
 
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The Analytical Chemistry of Silicones (Chemical Analysis: A Series of Monographs on Analytical Chemistry and Its Applications) [Hardcover]

A. Lee Smith (Editor)

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Book Description

0471516244 978-0471516248 January 18, 1991 1
High-Resolution Solid-State NMR of Silicates and Zeolites Gunter Engelhardt and Dieter Michel "I strongly recommend this book as an important reference for scientists concerned with the structural properties of siliceous materials." --Applied Spectroscopy This well-organized and up-to-date text gives a thorough account of the wide range of applications of multinuclear high-resolution solid-state NMR spectroscopy in silicate and zeolite science, with emphasis on the kinds of chemical information retrievable from NMR experiments. 1988 (0 471-91597-1) 485 pp. The Chemistry of Silica Solubility, Polymerization, Colloid and Surface Properties, and Biochemistry Ralph K. Iler A major component of the earth's solid surface and the constituent of sand, silica--an ageless natural staple--is also integral to industries as diverse as chemistry, biology, medicine, agriculture, metallurgy, and mining. This landmark reference details the chemistry surrounding the research and development of silica as well as information on its production and production control. 1979 (0 471-02404-X) 866 pp. The Chemistry of Organic Silicon Compounds Parts 1 and 2 Edited by Saul Patai and Zvi Rappoport "This volume will probably become the first reference consulted for C-Si chemistry." --Choice This authoritative account of organic compounds containing carbon-silicon bonds brings specialists up-to-date to the field's latest innovative turns. The emphasis in this compilation of studies--from 17 prominent researchers--is on small molecules, single bonds, analysis, structure, synthesis, spectroscopy, and reaction mechanisms. Part 1:1989 (0 471-91441-X) 892 pp. Part 2:1989 (0 471-91992-6) 1,668 pp.

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Editorial Reviews

From the Publisher

The fast paced developments in the field of silicone analytical chemistry over the last 15 years have been tremendous, and the explosion of knowledge during that time has been phenomenal. Updates the latest findings in the field and presents them in a concise, yet comprehensive manner. Principles and general approaches to problems are stressed, and examples cited of some of the typical approaches to problems of current interest, including: polymers and compositions; trace analysis; personal care applications; chromatographic methods; infrared, Raman, near-infrared and ultraviolet spectroscopy; nuclear magnetic resonance spectroscopy; mass spectrometry; and more. In addition, key references are cited for further reading.

From the Inside Flap

The new universe of innovative analytical techniques in chemistry—Fourier transform spectroscopy, near-infrared spectroscopy, a variety of surface analysis techniques, chemometrics and computerized instrumentation—has been matched in innovative velocity only by the phenomenal rise in uses for organosilicon materials. Indispensable as high-performance materials in industrial processes and products and in medical and biological applications, silicones offer a versatile new language for chemistry—whose syntax is understood through analytical technology. The Analytical Chemistry of Silicones is a guide to understanding the unique chemistry of organosilicon materials—a valuable compendium for chemists and engineers that covers techniques for analyzing, and analyzing for, organosilicon compounds. By frequently illustrating approaches with problems of current interest, the authors provide the reader with an up-to-the-minute glimpse into silicone chemistry’s full structural and analytical permutations. Inside, readers will find:
  • Methods of analyzing for silicones —from parts per billion to 100%, both in bulk materials and on surfaces
  • Analysis of products and formulations—from coatings and cosmetics to surfactants and textile treatments
  • Analysis for traces of silicones—in foods, soil, water, air, medical devices, and biological samples
  • Proven methods for analyzing organosilicon monomers and polymers for composition and structure
  • Experimental methods for determining physical properties and polymer structure
  • Microscopical characterization techniques—from optical to analytical electron microscopy
  • Chromatographic, NMR, IR, mass spectrometric, atomic spectroscopic, and X-ray methods, and other key techniques—with emphasis on their uses in characterizing silicones
  • Up-to-date tables of physical property data for many monomers and oligomers, GC response factors, IR group frequencies, and NMR shiftsA comprehensive bibliography of relevant literature citations, including titles
A synthesis of information and data heretofore unavailable in a single source, this first-of-a-kind resource allows chemical engineers or research chemists, analytical generalists, and analytical specialists—with varying degrees of familiarity with analytical chemistry or silicones—to become conversant with both the techniques of analysis and science of silicones, allowing for the swift and economical solution to analytical problems. Invaluable for its breadth of coverage and practical detail, The Analytical Chemistry of Silicones is the essential primer to the infinitely useful and unfolding chemistry of organosilicon materials.

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Inside This Book (learn more)
First Sentence:
When you can measure what you are speaking about and express it in numbers, you know something about it; but when you cannot express it in numbers, your knowledge is of a meagre and unsatisfactory kind; it may be the beginning of knowledge, but you have scarcely in your thoughts advanced to the state of science, whatever the matter may be. Read the first page
Key Phrases - Statistically Improbable Phrases (SIPs): (learn more)
organosilicon materials, boiling silanes, organosilicon surfaces, siloxy units, polymer surface dynamics, bond refractions, shift correlation chart, siliconium ion, organosilicon monomers, organosilicon compounds, additivity constants, organosilicon polymers, leveling bulb, organic silicon compounds, silicon analysis, ethoxy silanes, silane hydrogen, silanol condensation, siloxane polymers, personal care applications, scanning electron microprobe, volatile silicones, silicone materials, organosilicon chemistry, silicon backbone
Key Phrases - Capitalized Phrases (CAPs): (learn more)
New York, Dow Corning Corporation, Plenum Press, American Chemical Society, John Wiley, Lee Smith, Karl Fischer, The Chemistry of Organic Silicon Compounds, Mass Spectrom, Marcel Dekker, Colloid Interface Sci, Cornell University Press, High Resolut, Pergamon Press, San Francisco, Courtesy Academic Press, Total Environ, Compound Retention Index Estimated, Principles of Polymer Chemistry, Acta Chem, Annual Book of Standards, Division of Polymer Chemistry, Interface Anal, Kynoch Press, Shreedhara Murthy
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