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GC/MS: A Practical User's Guide
 
 
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GC/MS: A Practical User's Guide [Hardcover]

Marvin McMaster (Author)
2.7 out of 5 stars  See all reviews (3 customer reviews)

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Book Description

0470101636 978-0470101636 February 8, 2008 2
Updated and expanded, the classic guide to GC/MS helps chromatographers quickly learn to use this technique for analyzing and identifying compounds. After explaining the fundamentals, it discusses optimizing, tuning, using, and maintaining GC/MS equipment; explores advances in miniaturized and field-portable GC/MS systems and microfluidic components; and more. Complete with a CD-ROM, it covers applications in the environmental laboratory and in forensics, toxicology, and space science. This is the premier resource for professionals in those fields and for students.

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Editorial Reviews

From the Publisher

Gas chromatography/mass spectrometry (GC/MS) is a highly popular analytical system used by organic chemists and analytical chemists in research and in professional analytical labs, including environmental labs. It is used to separate, identify, and quantify individual compounds and substances. Chromatography was used to identify the ingredients of the World Trade Center bomb and was one the main reasons for the quick arrest of the suspects. This book provides information on using, maintaining, and troubleshooting analytical instrument systems in operations laboratories. It contains practical tips based on actual experience, and only enough theory to show the operational variables and how to control them. Readers will gain an understanding of the components in their systems and get them up and running more rapidly. --This text refers to an out of print or unavailable edition of this title.

From the Back Cover

The classic guide to GC/MS—now expanded and updated

The combination of gas liquid chromatography (GC) for separation and mass spectrometry (MS) for detection and identification of the components of a mixtureof compounds is rapidly becoming the definitive analytical tool in research and commercial analytical laboratories. GC/MS: A Practical User's Guide, Second Editionis a concise primer for the novice chromatographer who needs to get up to speed on using this technique to analyze and identify compounds for various applications. After chapters that explain the essential principles, this authoritative guide:

  • Discusses the practical aspects of optimizing, tuning, using, and maintaining GC/MS equipment

  • Explores recent advances in miniaturized and field-portable GC/MS systems and microfluidic components

  • Covers applications in the environmental laboratory and in forensics, toxicology, and space science

  • Features information on using spectral databases for identifying compounds

  • Includes a CD-ROM with a PowerPoint® slide set, FAQs, tables, and a glossary

This is the reliable, hands-on resource on GC/MS for organic, analytical, clinical, environmental, and forensic chemists in all types of laboratories, as well as for students in these specialties.


Product Details

  • Hardcover: 192 pages
  • Publisher: Wiley-Interscience; 2 edition (February 8, 2008)
  • Language: English
  • ISBN-10: 0470101636
  • ISBN-13: 978-0470101636
  • Product Dimensions: 6.5 x 0.8 x 9.5 inches
  • Shipping Weight: 1 pounds (View shipping rates and policies)
  • Average Customer Review: 2.7 out of 5 stars  See all reviews (3 customer reviews)
  • Amazon Best Sellers Rank: #1,338,191 in Books (See Top 100 in Books)

More About the Author

Dr. Marvin McMaster is a full-time writer, adjunct professor of Chemistry at the U. Missouri-St. Louis teaching seminars and short extension course on laboratory instruments, selling, and computers, and teaches Bible study at his local Methodist church.

He currently works as a consultant from the St.Louis area, teaches at St. Andrew UMC in Florissant, MIssouri, and is extending his writing into World War II biography, religious fiction and non-fiction. and science fiction/fantasy after having accidentally encountered the royal wishing pig, Aloysius.

His latest published work "Buying and Selling Laboratory Instruments" is dual purposed. It provides a guide to the purchasing process by a knowledgeable sales specialist unconnected to manufacturers. It also represents the first systematic guide to the selling profession by a successful Win-Win salesman who has made a career out of making customer's successful with their instruments.

TANSTAAFL applies to selling as well as to life. "There ain't no such thing as a free lunch!" A salesman who fails to make his customers successful with his products is going to starve to death because he never gets any repeat business. Judge Ziglar was right when he said, "Timid Salesmen Have Skinny Kids." So do salesman who do not support and make their customer successful.

Dr. McMaster has a Ph.D. in Organic Chemistry from the U. Nebraska-Lincoln, laboratory experience as a synthetic and process chemist with DuPont, Kraft Foods, Ciba-Geigy and biochemical/medical postdoctoral experience at Florida State U., U. Colorado Med. School, and U. Michigan. For 25 years he sold laboratory instruments and computer interfaces as a technical sales representative for Waters Associates, LDC, Beckman Instruments, Pharmacia/LKB, and Teknivent. He has also worked as a networking and support technician for MacIntosh computer at Washington U. Medical School in St. Louis.

He began teaching 2-day in-field HPLC courses for Beckman and added evening extensions courses at UMSL and wrote his first book "HPLC: A Practical User's Guide" when he was unable to find a useable textbook. Laboratory computers. GC/MS and LC/MS courses and books were added as this expertise emerged from his selling career.


 

Customer Reviews

3 Reviews
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Average Customer Review
2.7 out of 5 stars (3 customer reviews)
 
 
 
 
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Most Helpful Customer Reviews

14 of 16 people found the following review helpful:
3.0 out of 5 stars Good Introduction to GC-MS, January 1, 2002
By 
GC/MS should be helpful to the novice or student who has never used GC-MS before and who has had minimal experience with GC. It is a little disappointing that about 20% of the text covers material about GC that any experienced GC user should already know.
The book contains an easy to understand explanation about how a mass spectrometer works. Some additional details or diagrams could have clarified the description of how the DC/RF field separates the mass fragments in the quadrupole analyzer; but otherwise the text is crystal clear. Information about tuning and maintaining the mass spectrometer is well presented and the authors provide some helpful suggestions including a way to tell during the tuning process that the source needs cleaning. More information about spectral interpretation would have been appreciated but is probably outside the scope of the book.
This book belongs on the library shelves of colleges with undergraduate chemistry programs and would be helpful in industrial and environmental laboratories as an introduction for chemists and technicians new to the field.
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3 of 3 people found the following review helpful:
1.0 out of 5 stars Out of date and incorrect - avoid, December 4, 2008
By 
This review is from: GC/MS: A Practical User's Guide (Hardcover)
For a book that has been through a number of revisions over several years one would expect accuracy, credibility and efficacy. Sadly this book fails on every count. It starts by listing the masses of simple molecules incorrectly (O2 = 34) and continues with poorly drawn diagrams and overly wordy explanation. I can find little up to date in this 'new' release, it really is just a poor rehash of dated material.

As an experienced mass spectrometrist I hoped this book word serve as a nice introduction to the field of GC/MS for new staff. Sadly it was received by new colleagues as dated and with little credibility.

Save yourself $60 and try Wikipedia instead.
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7 of 10 people found the following review helpful:
4.0 out of 5 stars Fantastic list of tips for a GC/MS user, February 12, 2000
The book may be considered difficult for a starting user. I have been working with GC/MS for 10 years and the coments and all explanations inside are really and absolutely useful. Unfortunately I had not such a book when I was starting to deal with this technique.
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Inside This Book (learn more)
Key Phrases - Statistically Improbable Phrases (SIPs): (learn more)
cal gas valve, throat liner, tuning compound, ceramic collars, mass spectrometer source, exit electrode, volatile organic analysis, purge tube, mass spectrometer interface, rough pump, quadrupole rods, primary fragments, linear ion trap, secondary fragments, calibration gas, turbo pump, oil diffusion pump, quadrupole analyzer, compressed area, ion fragments, ion detector, fragmentation data
Key Phrases - Capitalized Phrases (CAPs): (learn more)
Second Edition, Practical User's Guide, John Wiley, Target Compounds Compound Retention
Browse Sample Pages:
Front Cover | Table of Contents | First Pages | Index | Surprise Me!
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