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Organic Structures from Spectra [Paperback]

Leslie D. Field (Author), Sev Sternhell (Author), John R. Kalman (Author)
4.0 out of 5 stars  See all reviews (4 customer reviews)

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Book Description

0470319275 978-0470319277 March 11, 2008 4
Organic Structures from Spectra, Fourth Edition consists of a carefully selected set of over 300 structural problems involving the use of all the major spectroscopic techniques. The problems are graded to develop and consolidate the student’s understanding of Organic Spectroscopy, with the accompanying text outlining the basic theoretical aspects of  major spectroscopic techniques at a level sufficient to tackle the problems.

Specific changes for the new edition will include

  • A significantly expanded section on 2D NMR spectroscopy focusing on COSY, NOESY and CH-Correlation
  • Incorporating new material into some tables to provide extra characteristic data for various classes of compounds
  • Additional basic information on how to solve spectroscopic problems
  • Providing new problems within the area of 10 2D NMR spectroscopy
  • More problems at the ‘simpler’ end of the range

As with previous editions, this book combines basic theory, practical advice and sensible approaches to solving spectra problems. It will therefore continue to prove invaluable to students studying organic spectroscopy across a range of disciplines.


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Editorial Reviews

Review

"This volume...consists of?structural problems based on major spectroscopic techniques and...problems that deal specifically with the interpretation of spin-spin coupling..." (Spectroscopy, Vol. 17, No. 12, December 2002) --This text refers to an out of print or unavailable edition of this title.

From the Back Cover

The derivation of structural information from spectroscopic data is now an integral part of organic chemistry courses at all Universities. A critical part of any such course is a suitable set of problems to develop the student’s understanding of how structures are determined from spectra.

Organic Structures from Spectra, FourthEditionis a carefully chosen set of more than 280 structural problems employing the major modern spectroscopic techniques, a selection of 18 problems using 2D-NMR spectroscopy, more than 20 problems specifically dealing with the interpretation of spin-spin coupling in proton NMR spectra and 8 problems based on the quantitative analysis of mixtures using proton and carbon NMR spectroscopy. All of the problems are graded to develop and consolidate the student’s understanding of organic spectroscopy. The accompanying text is descriptive and only explains the underlying theory at a level which is sufficient to tackle the problems. The text includes condensed tables of characteristic spectral properties covering the frequently encountered functional groups.

The examples themselves have been selected to include all important structural features and to emphasise connectivity arguments. Many of the compounds were synthesised specifically for this purpose. There are many more easy problems, to build confidence and demonstrate basic principles, than in other collections. 

The fourth edition of this popular textbook:

  • now incorporates a suite of new problems dealing with the analysis of 2D NMR spectra (COSY, NOESY, TOCSY and C‑H Correlation spectroscopy);
  • has been expanded and updated to reflect the new developments in the area;
  • has an additional 25 carefully selected basic problems;
  • provides a set of problems dealing specifically with the quantitative analysis of mixtures using NMR spectroscopy;
  • features proton NMR spectra obtained at 200, 400 and 600 MHz and 13C NMR spectra include DEPT experiments as well as proton-coupled experiments;
  • conatins 6 problems in the style of the experimental section of a research paper and the appendix contains examples of fully worked solutions.

Organic Structures from Spectra, Fourth Edition will prove invaluable for students of Chemistry, Pharmacy and Biochemistry taking a first course in Organic Chemistry.

Review from earlier edition

"…I would definitely state that this book is the most useful aid to basic organic spectroscopy teaching in existence and I would strongly recommend every instructor in this area to use it either as a source of examples or as a class textbook."
—Magnetic Resonance in Chemistry


Product Details

  • Paperback: 468 pages
  • Publisher: Wiley; 4 edition (March 11, 2008)
  • Language: English
  • ISBN-10: 0470319275
  • ISBN-13: 978-0470319277
  • Product Dimensions: 11.6 x 8.3 x 1.1 inches
  • Shipping Weight: 3 pounds (View shipping rates and policies)
  • Average Customer Review: 4.0 out of 5 stars  See all reviews (4 customer reviews)
  • Amazon Best Sellers Rank: #74,101 in Books (See Top 100 in Books)

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3 of 4 people found the following review helpful:
3.0 out of 5 stars It's a good supplement, April 8, 2000
By A Customer
I had to buy this book for a Spectroscopy class, and I came to Amazon looking to see if there is an answer book too (which i don't think exists). Don't let the book discription fool you... The questions are "graded" meaning they progressively get more difficult. The questions are NOT answered, which would have been very helpful. If you are looking for a VERY BASIC explination to spectral chemistry, and a bunch of problems, get this book. If you want to really know what spectral chem is all about try "Spectrometric Identification of Organic Compounds".
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4.0 out of 5 stars :-), April 15, 2010
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Amazon Verified Purchase(What's this?)
This review is from: Organic Structures from Spectra (Paperback)
I got this book for a class. The problems in the book were much easier and gave much more information than the problems on my exams (or for real life) but it was a good book. The problems give you more hints (like MW) than you would truly get from identifying a real spectra or (for some of you) on an exam.
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4.0 out of 5 stars Great Book!, February 7, 2009
By 
Sean Ross "Chem Nerd" (Biggest little City,USA) - See all my reviews
(REAL NAME)   
This review is from: Organic Structures from Spectra (Paperback)
This is a great book, I bought this book for a organic spectra and structure class and loved it. The problems are fun. I like to think of them as a chemistry sudoku. Any student that wants to get into Ochem needs this book!
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Inside This Book (learn more)
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First Sentence:
The basic principles of absorption spectroscopy are summarised below. Read the first page
Key Phrases - Statistically Improbable Phrases (SIPs): (learn more)
proton decoupled solvent, ppm expansion, ppm proton decoupled, coupled proton decoupled, ppm exchanges, relevant coupling constants, hybridised carbon atoms, splitting diagram, solvent expansions, schematic spectrum, ppm solvent, mass spectrum, nujol mull, stereogenic centre, characteristic chemical shifts, protonated carbons, attached protons, chemical shift range, polynuclear aromatic compounds, aromatic region, liquid film, above spectrum, aromatic protons
Key Phrases - Capitalized Phrases (CAPs): (learn more)
Spectrum Xmax
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