The book is intended for an audience already familiar with proton and carbon NMR and commencing research in phosphane chemistry (broadly defined). It is the primary aim of this book to enable the reader to identify the main factors governing the phosphorus chemical shift values in the 31P-NMR spectrum and to make an educated guess as to where the phosphorus resonance(s) of a given target compound can be expected. It is not within the scope of this book to enable one to predict a phosphorus chemical shift precisely or even within a reasonable margin of error, with a few notable exceptions. The further intent of this book is to assist the reader in determining important issues like bond order, p-bonding contributions from substituents, the existence or non-existence of metallacycles etc., in short, to make structural assignments without the aid of X-ray crystal structure determinations and to explain structural differences in solution and the solid state where appropriate.
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Aus den Rezensionen: "... ein kompaktes Lehrbuch zur Phosphor-31-NMR-Spektroskopie. Aufbauend auf Grundwissen, das der Leser zu NMR ... haben muss, werden ... die spezifischen Eigenheiten des Phosphorkerns erläutert. ... Das Gewicht des Buches liegt eindeutig auf einer klaren und exakten, gut lesbaren Einführung zu den unterschiedlichsten Phosphorhaltigen organischen Verbindungen. Hier muss anerkannt werden, dass der Autor eine grosse Bandbreite an Strukturen und Komplexen und die Auswirkungen auf die chemische Verschiebung sehr gut bespricht. ... Die unterschiedlichen Kopplungen werden ... gut erklärt und Werte für Kopplungen im Text erwähnt ..." (http://www.organische-chemie.ch/buecher/besprechungen/3540791175.shtm)
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Key Phrases - Statistically Improbable Phrases (SIPs):
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transition metal complexes, naked phosphorus, exocyclic phosphorus atom, phosphorus resonance, coordination chemical shift, phosphino amine, net upfield shift, upfield end, phosphorus chemical shift, expected downfield shift, phosphenium cations, primary phosphanes, observed downfield shift, tertiary phosphanes, significant upfield shift, phosphinidene complex, significant downfield shift, phosphino group, transition metal fragment, phosphane ligands, chemical shift values, isolobal relationship, donor bond, coupling constant increases, shifted downfield Key Phrases - Capitalized Phrases (CAPs): (learn more)
Organomet Chem, Inorg Chem, Chem Soc, Range of Chemical Shifts, Dalton Trans, Chem Comm, Springer-Verlag Berlin Heidelberg, Coord Chem Rev, Chem Ber, Angew Chem, Anorg Allg Chem, Chem Eur, Phosphorus Element Single Bonds, L'-Phosphanes Fig, Box Story, Phosphorus Phosphorus Bonds, Phosphorus Carbon Multiple Bonds Browse Sample Pages:
Front Cover | Table of Contents | First Pages | Index | Surprise Me!
transition metal complexes, naked phosphorus, exocyclic phosphorus atom, phosphorus resonance, coordination chemical shift, phosphino amine, net upfield shift, upfield end, phosphorus chemical shift, expected downfield shift, phosphenium cations, primary phosphanes, observed downfield shift, tertiary phosphanes, significant upfield shift, phosphinidene complex, significant downfield shift, phosphino group, transition metal fragment, phosphane ligands, chemical shift values, isolobal relationship, donor bond, coupling constant increases, shifted downfield Key Phrases - Capitalized Phrases (CAPs): (learn more)
Organomet Chem, Inorg Chem, Chem Soc, Range of Chemical Shifts, Dalton Trans, Chem Comm, Springer-Verlag Berlin Heidelberg, Coord Chem Rev, Chem Ber, Angew Chem, Anorg Allg Chem, Chem Eur, Phosphorus Element Single Bonds, L'-Phosphanes Fig, Box Story, Phosphorus Phosphorus Bonds, Phosphorus Carbon Multiple Bonds Browse Sample Pages:
Front Cover | Table of Contents | First Pages | Index | Surprise Me!
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