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Principles of Instrumental Analysis Hardcover – December 6, 2006

ISBN-13: 978-0495012016 ISBN-10: 0495012017 Edition: 6th

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Product Details

  • Hardcover: 1056 pages
  • Publisher: Cengage Learning; 6 edition (December 6, 2006)
  • Language: English
  • ISBN-10: 0495012017
  • ISBN-13: 978-0495012016
  • Product Dimensions: 10.3 x 8.4 x 1.6 inches
  • Shipping Weight: 4.4 pounds (View shipping rates and policies)
  • Average Customer Review: 3.4 out of 5 stars  See all reviews (48 customer reviews)
  • Amazon Best Sellers Rank: #78,799 in Books (See Top 100 in Books)

Editorial Reviews

Review

1. Introduction. Section I. MEASUREMENT BASICS. 2. Electrical Components and Circuits. 3. Operational Amplifiers in Chemical Instrumentation. 4. Digital Electronics and Microcomputers. 5. Signals and Noise. Instrumental Methods in Action: Assessing the Authenticity of the Vinland Map. Section II. ATOMIC SPECTROSCOPY. 6. An Introduction to Spectrometric Methods. 7. Components of Optical Instruments. 8. An Introduction to Optical Atomic Spectrometry. 9. Atomic Absorption and Atomic Fluorescence Spectrometry. 10. Atomic Emission Spectrometry. 11. Atomic Mass Spectrometry. 12. Atomic X-Ray Spectrometry. Instrumental Methods in Action: Title. Section III. MOLECULAR SPECTROSCOPY. 13. An Introduction to Ultraviolet/Visible Molecular Absorption Spectrometry. 14. Applications of Ultraviolet/Visible Molecular Absorption Spectrometry. 15. Molecular Luminescence Spectrometry. 16. An Introduction to Infrared Spectrometry. 17. Applications of Infrared Spectrometry. 18. Raman Spectroscopy. 19. Nuclear Magnetic Resonance Spectroscopy. 20. Molecular Mass Spectrometry. 21. Surface Characterization by Spectroscopy and Microscopy. Instrumental Methods in Action: Title. Section IV. ELECTROANALYTICAL CHEMISTRY. 22. Introduction to Electroanalytical Chemistry. 23. Potentiometry. 24. Coulometry. 25. Voltammetry. Instrumental Methods in Action: Title. Section V. SEPARATION METHODS. 26. An Introduction to Chromatographic Separations. 27. Gas Chromatography. 28. High-Performance Liquid Chromatography. 29. Supercritical Fluid Chromatography and Extraction. 30. Capillary Electrophoresis and Capillary Electrochromatography. Instrumental Methods in Action: Title. Section VI. MISCELLANEOUS METHODS. 31. Thermal Methods. 32. Radiochemical Methods. 33. Automated Methods of Analysis. 34. Particle Size Analysis. Instrumental Methods in Action: Title. Appendices. Appendix 1. Evaluation of Analytical Data. Appendix 2. Some Standard and Formal Electrode Potentials. Appendix 3. Compounds for Preparing Standard Solutions of Some Common Elements. Appendix 4. Common Acronyms Encountered in Chemical Instrumentation. Answers to Selected Problems. Index.

About the Author

Douglas A. Skoog (deceased) earned a B.S. in chemistry from Oregon State University and received his Ph.D. in analytical chemistry from the University of Illinois. The lead author of several best-selling texts, Dr. Skoog was the 1999 recipient of the American Chemical Society award in analytical chemistry, sponsored by the Fisher Scientific Company. That same year, he was named a Fellow of the American Association for the Advancement of Science. In 1993, he received the ACS Division of Analytical Chemistry Award for Excellence in Teaching. He was a Professor of Chemistry at Stanford University.

F. James Holler is a Professor of Chemistry and recipient of the Alumni Association Great Teacher Award at the University of Kentucky. He received his Ph.D. from Michigan State University. In addition to his role as co-author of several best-selling texts, he is co-creator of the world-famous Periodic Table of Comic Books.

Stanley R. Crouch is Professor Emeritus at Michigan State University. He received his undergraduate and M.S. degrees from Stanford University and his Ph.D. in analytical chemistry from the University of Illinois. He is the recipient of the 2001 American Chemical Society Division of Analytical Chemistry Award in Chemical Instrumentation and the 1996 ACS Division of Analytical Chemistry Award for Excellence in Teaching.

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Customer Reviews

Without at least a decent professor, a student using this text would not gain very much.
Ryne Johnston
What's sold was an international edition and bad quality the book pages as falling apart.
Patricia Tortosa
A great learning experience for an undergrad and a great review for any graduate student.
Wade

Most Helpful Customer Reviews

20 of 20 people found the following review helpful By A.Reader1 on March 8, 2007
Format: Hardcover
I'm not sure why there are so many negative reviews of this book. I found it to be very solid when I used the 3rd edition.

For those of you who don't like it you have 4 options:

1. "Instrumental Methods of Analysis" by Willard, Merritt, Dean, Settle; (ISBN 0534081428) which is excellent and a true classic. It's OOP now but a new edition comes out in 2016.

2. "Chemical Analysis: Modern Instrumentation Methods and Techniques" by Francis Rouessac & Annick Rouessac

3. "Undergraduate Instrumental Analysis" Sixth Edition by James W. Robinson, Eileen M. Skelly Frame, George M. Frame II

4. "Chemical Instrumentation: A Systematic Approach" by Strobel and Heineman. This book is very hardware oriented and is not a true general instrumental analysis text.

I'd also recommend that you buy "Statistics and Chemometrics for Analytical Chemistry" by James N. Miller & Jane C. Miller. It does a much better job than the cursory chapters found in regular analytical texts. Get the 4th or 5th edition. For a paperback, this book is ridiculously expensive if you buy new. Try to find a used copy.

While the book by Miller & Miller is good, it's no substitute for a 1 or 2 semester course in stats. A good book for this material might be Statistics for Research, Third Edition by Shirley Dowdy, Stanley Wearden, Daniel Chilko (ISBN 047126735X)

Check out my other reviews for other undergrad. chem books.

I notice one of the co-authors (Crouch) has added his comments. He says "This book remains the leader in the field." - not difficult when there are so few competitors!
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4 of 4 people found the following review helpful By C. Myslinski on September 17, 2007
Format: Hardcover Verified Purchase
I have to use this textbook for one of my classes, and I must say, it is horrible. The examples for problems in the book hardly give any explanation of what they are doing. The questions at the end of the chapter are very difficult and looking back at the chapter just makes the question even more confusing. I like to use textbooks when I do not understand what is going on in my class, but this one does not help at all! I think the only way you can understand this book is if you are already well educated in the course. Everytime I am assigned problems in the book, I cringe, because I know I am going to be spending hours being more confused than I have ever been in my life.
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3 of 3 people found the following review helpful By N. Simon on December 6, 2008
Format: Hardcover Verified Purchase
I used this textbook for an instrumental analysis class. It is very informative and contains helpful schematics and figures to enhance the text material. That being said, it often is a very dense read. I had issues being able to comprehend more than a couple pages in one sitting.
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3 of 3 people found the following review helpful By KJ on April 9, 2009
Format: Hardcover
There are too many errors in problems and solutions that it does more harm to people like me who learn by examples. I also hate how it has incorrectly spelled words in glossary section.
I wonder if the authors ever proofread this book?
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2 of 2 people found the following review helpful By V. Gu on October 7, 2010
Format: Hardcover
I found the organization of the subject material very disorganized. I found myself at times referring to later chapters to understand what was being said in the current chapter. The questions had the same problem. In one particular chapter, I had to refer back several chapters to do the problems. Normally this is not an issue, but these particular problems would have been better suited for the chapter the concept/equation was first introduced... not 7 chapters later.
There were also numerous errors and typos.
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2 of 2 people found the following review helpful By MJJPW on March 1, 2011
Format: Hardcover Verified Purchase
Great content, but a little lengthy making it difficult to find exactly what you are looking for. Very complete and expanded explainations. Great for an analytical lab.
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1 of 1 people found the following review helpful By J. Gualco on November 5, 2007
Format: Hardcover
This is definately not the best textbook in the world. It is excrutiatingly detailed and does not easily guide you through the material, helping you to learn it. On the other hand, its detail is what makes it a phenomenal reference book. In it you can find not only vast amounts of information on your topic, but also references to aid you in researching it further.

I admit it. I couldn't use this book at all when I first started my analysis class but now it has become an invaluable tool in my research and a key in my reference library.
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1 of 1 people found the following review helpful By Bryce P Rasmussen on October 13, 2008
Format: Hardcover
Well, as far as this book goes...it sucks. While it is written in a language most chemistry/analytical students can understand, there is no summary of the instruments without going into excruciating and mostly useless detail. Great reference books for Ph. D's who need an actual reliable, specific book. Not worth the price - get the International Student Edition for $40 - it's exactly the same, even thought it says it MAY not be the same, it is.
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