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Purification of Laboratory Chemicals, Fifth Edition
 
 
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Purification of Laboratory Chemicals, Fifth Edition [Paperback]

Christina Chai (Author), W.L.F. Armarego (Author)
4.0 out of 5 stars  See all reviews (5 customer reviews)


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Paperback, April 3, 2003 --  
There is a newer edition of this item:
Purification of Laboratory Chemicals, Sixth Edition Purification of Laboratory Chemicals, Sixth Edition 4.0 out of 5 stars (5)
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Book Description

0750675713 978-0750675710 April 3, 2003 5
Now in its fifth edition, the book has been updated to include more detailed descriptions of new or more commonly used techniques since the last edition as well as remove those that are no longer used, procedures which have been developed recently, ionization constants (pKa values) and also more detail about the trivial names of compounds.

In addition to having two general chapters on purification procedures, this book provides details of the physical properties and purification procedures, taken from literature, of a very extensive number of organic, inorganic and biochemical compounds which are commercially available. This is the only complete source that covers the purification of laboratory chemicals that are commercially available in this manner and format.

* Complete update of this valuable, well-known reference
* Provides purification procedures of commercially available chemicals and biochemicals
* Includes an extremely useful compilation of ionisation constants


Editorial Reviews

Review

Review of previous edition:

This monograph remains the bible for practising chemists wishing to know how to dry solvents or purify commercially available laboratory chemicals...The authors have made good use of computerised databases for up to date information and have placed a noticeable emphasis on safety. It is of manageable size and, like its forebears, will be the most commonly used reference book in any chemical or biochemical laboratory. - Molecular Diversity Preservation International (MDPI), October 1997

Book Description

Purification of Laboratory Chemicals is vital for minimizing potentially dangerous reactions, as well as maximizing the integrity of chemicals used to process a product that must adhere to rigorous scientific standards.

Product Details

  • Paperback: 608 pages
  • Publisher: Butterworth-Heinemann; 5 edition (April 3, 2003)
  • Language: English
  • ISBN-10: 0750675713
  • ISBN-13: 978-0750675710
  • Product Dimensions: 11.3 x 8.1 x 1.6 inches
  • Shipping Weight: 4.1 pounds
  • Average Customer Review: 4.0 out of 5 stars  See all reviews (5 customer reviews)
  • Amazon Best Sellers Rank: #1,714,575 in Books (See Top 100 in Books)

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Average Customer Review
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19 of 20 people found the following review helpful:
4.0 out of 5 stars Great for the Organic Chemist, December 31, 1998
Like Carey & Sundberg, Jerry March, the Aldrich catalog, and the Merck Index, (etc.), this book should be a benchmate for the Organic Chemist. It is very good when one requires the purification of reagents, or the drying/purification of solvents. The protocols for purification are usually pretreatment followed by distillation or recrystallization, and can be carried out to give anywhere from moderately pure material, to giving the pure, pure substance.

Excellent for the research organic chemistry graduate student or the pharmaceutical industrial research chemist who likes to start with the purest materials, so as to leave only the investigative variables open to question.

However, in industry, although FedEx-ing new and pure reagents (and disposal of the old questionable ones!) is the easiest and encouraged method for research, it is often found that purification is totally appropriate--in these instances, Purification of Laboratory Chemicals (D.D. Perrin & W.L.F. Armarego) is highly recommended.

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11 of 11 people found the following review helpful:
4.0 out of 5 stars An Absolute Essential for Chemists!, November 17, 2000
As a chemist, I am often in need of techniques for purification of various chemicals. Often time is a constraint and the "best" technique may be too time consuming, if one even knows what it is. This text offers several alternatives to the purificatin of most common compounds (especially solvents), including the best way to make the compound pure as well as other known techniques. One can then choose, based on the reaction one is doing whether one needs to use the best techniques or the fastest technique to get mostly pure material or somewhere inbetween. Unfortunately, often the text does not list the actual percent purity that each technique can yield (though it is often easy enough to guess which methodology will yield the best results.) An invaluable resource for any chemist, but especially for graduate students.
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5 of 6 people found the following review helpful:
5.0 out of 5 stars Great for the "Synthetic" Chemist, June 5, 2000
By 
Craig MACKINNON (Thunder Bay, Ontario Canada) - See all my reviews
This is an indispensible resource for any synthetic chemist, either organic or inorganic (not sure about the biochemical section). This book has concise, informative entries on the purification of a vast number of common solvents and reagents. I don't know how any chemist can survive without having this on his/her bookshelf!
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Inside This Book (learn more)
First Sentence:
Purity is a matter of degree. Read the first page
Key Phrases - Statistically Improbable Phrases (SIPs): (learn more)
fractional distn, distd water, vacuum distd, white ppte, pet ether, vac desiccator, ether soln, saturated aqueous soln, distil under vacuum, wash with aqueous, ppm resp, glass helices, alumina before use, olefinic impurities, alkaline soln, distillate solidifies, soln containing, efficient fume cupboard, been recrystallised, likely impurities, fractional freezing, acid crystallises, first coloration, hot glacial acetic acid, saturated soln
Key Phrases - Capitalized Phrases (CAPs): (learn more)
Chem Soc, Org Chem, Chem Ber, Phys Chem, Biol Chem, Anal Chem, Org Synth Coll Vol, Justus Liebigs Ann Chem, New York, Heiv Chim Acta, Hely Chim Acta, Tetrahedron Lett, Faraday Trans, Biochem Prep, Anal Biochem, Acta Chem Scand, Methods Enzymol, Inorg Synth, Handbook of Preparative Inorganic Chemistry, Chem Commun, Trans Faraday Soc, Biochim Biophys Acta, Chem Ind, Appl Chem, Dalton Trans
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