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Quantitative Chemical Analysis Hardcover – April 30, 2010

ISBN-13: 978-1429218153 ISBN-10: 1429218150 Edition: Eighth Edition

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Product Details

  • Hardcover: 750 pages
  • Publisher: W. H. Freeman; Eighth Edition edition (April 30, 2010)
  • Language: English
  • ISBN-10: 1429218150
  • ISBN-13: 978-1429218153
  • Product Dimensions: 11 x 9.3 x 1.4 inches
  • Shipping Weight: 5.1 pounds (View shipping rates and policies)
  • Average Customer Review: 4.2 out of 5 stars  See all reviews (61 customer reviews)
  • Amazon Best Sellers Rank: #19,507 in Books (See Top 100 in Books)

Editorial Reviews

About the Author

Biographical Statement for Nomination of Daniel C. Harris for
J. Calvin Giddings Award for Excellence in Analytical Chemical Education
I was born in 1948 in Brooklyn, New York.  As a teenager, I enjoyed a science program on Saturdays at Columbia University, where I took note of especially good teaching by astronomy professor Lloyd Motz.  In my freshman year at Massachusetts Institute of Technology, excellent teaching of organic chemistry by Daniel S. Kemp diverted me from biochemistry to chemistry.  A spectroscopy class from George F. Whitesides led me to Whitesides and his student Chuck Casey (later President of the American Chemical Society) for senior thesis research.  I developed a strong consciousness for high quality teaching.  Two other classes with noteworthy teaching quality were quantum mechanics from John S. Waugh and group theory from F. A. Cotton.

After graduating from MIT shortly before my 20th birthday, I headed to Caltech where I joined the research group of Harry B. Gray—an exceptional lecturer.  After a year as a teaching assistant in organic chemistry, George S. Hammond and Harry Gray recognized a spark for teaching and offered me the opportunity to team teach an advanced freshman course.  My graduate student partner, Michael D. Bertolucci, and I were given carte blanche to develop an interesting course for freshman that would not overlap other courses in the curriculum.  We chose an overview of general chemistry for one term, followed by two terms of introduction to group theory and spectroscopy.  We conducted a critique of each other’s lecture immediately after every class.  I placed highest value in interest, content, clarity, and physical understanding, which became main goals in my textbook writing.  At the age of 21, I found myself driven to write lecture notes which, upon the recommendation of Harry Gray, evolved into the book Symmetry and Spectroscopy.  I team-taught the freshman course with other graduate students and had the academic rank of Instructor during my last year of graduate studies.  For part of that year, I was a postdoc in the fledgling field of 13C-NMR spectroscopy with John D. Roberts.

After two years as a postdoc at the Albert Einstein College of Medicine in New York City with Philip Aisen—an exemplary mentor—I started my first faculty position at the University of California at Davis in 1975.  I was assigned to teach analytical chemistry for sophomores and accelerated freshmen.  This assignment was interesting because I had never taken a course in analytical chemistry.  I arrived at MIT after analytical chemistry became an elective and flew through MIT too quickly to partake in the analytical course.  I had practical analytical experience from undergraduate, graduate, and postdoctoral research.  My source of instruction in chemical equilibrium was the graduate course “Aquatic Chemistry” taught by J. J. Morgan at Caltech.  At Davis, I sat in on an analytical courses taught by a senior member of the department to “learn the ropes” before being thrust before my first students in analytical chemistry.

My burning desire at Davis was to be the best teacher I could be.  I was known for being available at all hours for student questions, for circulating through laboratories every day, and for memorizing the names and faces of every student.  It became apparent to students that sitting in the back row of a 300-seat lecture hall did not offer immunity from being called upon by name to answer a question during lecture.  I brought a demonstration into almost every lecture and each term ended with a series of explosions.  The last class each term attracted far more students than were enrolled in the course.  The majority of my students at Davis were life science majors whose interests resonated with my research interest in metalloproteins.

I surveyed every analytical textbook I could find and taught from several.  I found the more thorough books to be dull and the more interesting books to be less thorough.  After two years, I decided to write text to accompany my lectures.  My goal was to be interesting and thorough in the selected topics.  Publisher’s representatives saw my notes in the bookstore and soon there were five offers for publication.  I visited each publisher and unashamedly adopted the best suggestions from each editor.  In 1978, I signed with W. H. Freeman as the publisher I thought would produce the nicest book.  After two more years of writing, a year of revision, and a year of production, the first edition of Quantitative Chemical Analysis was born in 1982.

By this time, I had not been offered tenure at Davis or at Franklin and Marshall College.  I loved teaching, but decided to try a different career.  In 1983, I moved to the U.S. Navy’s Michelson Laboratory at China Lake, California, where my present title is Senior Scientist.  In the course of 25 years with the Navy, I was elected an Esteemed Fellow and received a Top Navy Scientist award.  My research concerns transparent ceramic sensor windows.  I have been teaching a professional course in this subject several times each year since 1990 and wrote the monograph Materials for Infrared Windows and Domes, which is the standard reference in its field.

Meanwhile, Quantitative Chemical Analysis sold well enough for the publisher to invite me to prepare a 2nd edition.  I found myself with two full-time jobs—one for the Navy and a second as a textbook writer.  My wife Sally has been editorial assistant and proofreader on every book.  She produced all of the illustrations for Symmetry and Spectroscopy with a one-year-old watching over her shoulder.  Thirty years after signing our contract with Freeman, we are working on the 8th edition.  The book has had 12 foreign translations.

Our chief competitor, Doug Skoog (with coauthors West, Holler, and Crouch) had “big” and “little” books to serve two market levels.  Freeman asked me to write a small book to complement Quantitative Chemical Analysis, but I hesitated to go into competition with myself.  By 1995, we no longer had children in the house and the time was ripe for a “small” book.  My priorities for Exploring Chemical Analysis were to be (1) short, (2) interesting, and (3) elementary—in that order.  This book has now gone through 4 editions and 3 foreign translations.
A survey published in 2002 found that my two books were used in over half of the analytical chemistry courses in the United States.  [P. A. Mabrouk, Anal. Chem. 2002, 74, 269A.]  In 2008, Quantitative Chemical Analysis received the McGuffey Longevity Award from the Textbook and Academic Authors Association.

In my writing, I try to catch the reader’s attention and to convey excitement by illustrating each topic with interesting real-world examples.  I try to get to the heart of a topic with the minimum number of words.  It is good pedagogy to explain everything and not to assume prior knowledge on the part of the reader.  Heavy use of illustrations makes ideas more understandable and memorable.  Chapters are broken into short sections which are more digestable than long sections.  Recalling my own student days, I include answers to all problems at the back of the book.  Some teachers would rather have a set of problems without answers, but I have never heard a student complain about immediate feedback after working a problem.  An informal writing style and a little humor provide a relaxed tone.
Quantitative Chemical Analysis evolved over 30-years.  Spectrophotometry grew from one to three chapters as it moved from the middle of the book to the front and then to the middle again.  Chromatography expanded from two to four chapters as its importance grew.  Electrophoresis and mass spectrometry were added.  Quality assurance, sampling, and sample preparation were added and quality assurance increased in importance.  Computer programming projects were introduced in the second edition.  Spreadsheets appeared in the fourth edition and increased in each subsequent edition.  A spreadsheet-oriented chapter on advanced chemical equilibrium appeared in the seventh edition.  Uniform, high-interest opening vignettes appeared in the fourth edition.  Chapter 0 on the “analytical process” describing an actual student analysis of caffeine in chocolate appeared in the fifth edition.  Gravimetric analysis was demoted to the back of the book.  Electroanalytical chemistry decreased from five to four chapters.  Instructions for experiments moved to the web in the sixth edition to make room for growth in other subjects.

Exploring Chemical Analysis began with brevity as the first goal.  User feedback directed me to add several topics that had been rejected for the first edition.  These topics included activity coefficients, systematic treatment of equilibrium, EDTA and redox titration curve calculations, and an expanded discussion of spectrophotometry.  Placement of spectrophotometry early in the book did not fit well with many curricula, so the subject was moved back in the second edition.  The third edition increased emphasis on quality assurance, integrated mass spectrometry with chromatography, and introduced inductively coupled plasma-mass spectrometry.  Spreadsheets gradually increased in every edition.  A short “ask yourself” question with an answer at the end of every worked example appeared in the fourth edition.

The most common comment I receive from teachers can be paraphrased as “I love your book and I wish it weren’t so long.  And please add more on (fill in favorite topic).”  Kolthoff, Sandell, Mehan, and Bruckenstein wrote in the preface of what was perhaps the most venerable analytical textbook of the 20th century, “as much as anyone, we regret the length of this revised edition ” (1170 pages) and “it is a very hard undertaking to seek to please everybody.”

A good textbook has the attributes of a good teacher.  The best description I have seen for a good teacher is a person with a “deep understanding of the subject, unbounded enthusiasm, humor, and the ability to communicate excitement, clarity and precision of thought and word, and the ability to put oneself in the mind of a student new to the subject.”  [C. Thyagaraja, Caltech News, 2000, 34[2], 11.]  To these I would add the ability to convey the significance and applications of the subject.  I strive toward these ends in my writing.

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Customer Reviews

The book was in mint condition.
Guy
To attest as how good this book is: Skoog's book was our main textbook while Harris was our supplement textbook.
A. T. Ko
The Good: This book was one of the most easy to understand chemistry books I have used throughout my career.
Julia Wilson

Most Helpful Customer Reviews

6 of 7 people found the following review helpful By Ion on September 17, 2010
Format: Loose Leaf Verified Purchase
From the start of the book, the reading isn't tedious and dreadful like most people think a book on chemistry would be. The 8th edition of Quantitative Chemical Analysis by Daniel C.Harris is very well written and actually engages you in the material! All the examples, pictures, and definitions are made for students who dread reading a chem book actually wanting to read and do the work inside it! Also, they have many examples of how to use Microsoft Excel to plot, e.g, Titration curves, plotting density, and how to make graphs. Overall, the book is great so far in my Analytical chem class and I plan on it helping me with all my lecture and lab materials
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3 of 3 people found the following review helpful By A.Reader1 on February 24, 2012
Format: Hardcover
since there are so many nonsense reviews of the 8th edition I thought I'd copy/paste my comments from the 7th edition:

So, you're considering either buying or adopting this text for intro analytical chemistry? Good choice!

This is the easiest, most straightforward, book on the market for students. It's been that way through many editions. It was a breath of fresh air (in comparison to Skoog) when it was first published in 1982.

Your other choices are "Fundamentals of Analytical Chemistry" by Skoog et al.(ISBN 0534417965) and "Analytical Chemistry" by Gary D. Christian (ISBN 0471214728). Can also use the book by Day & Underwood.

Skoog is good it's just that he can't match Harris for clarity.

Christian doesn't change much. The end-of-chapter problems are usually just re-numbered. It's OK, though.

Fortunately, whichever you choose, none can be considered deficient.

One thing I don't like about these books: Why do they include all this material on instrumental analysis? The advanced/Instrumental texts do a much better job with these topics anyway. The extra chapters make the intro books needlessly heavy.

The first course analytical books should just stick to the basics like acid/base/complexometric/redox titrations, gravimetric analysis, sample prep., extractions, etc.

----------------------------------------------------

Daniel Harris (along with Bertolucci) has also written a true classic in the field of molecular spectroscopy: "Symmetry and Spectroscopy: An Introduction to Vibrational and Electronic Spectroscopy". Get that too for your advanced phys chem courses.

Check out my other reviews for other chem books
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3 of 3 people found the following review helpful By A. T. Ko on June 29, 2011
Format: Hardcover
If you read through Harris' Quantitative Chemical analysis (8th edition), you will find that the topics covered are same as to what Skoogs' Fundamentals of Analytical Chemistry Book (8th edition)...the difference? READABILITY- while Skoogs can get very ambiguous to his formulation and how he calculates some examples (especially in acid-base titration and statistical analysis part), I fin that this where Harris' writing style and unassuming-you-know-everything pedagogy really shines in helping understand the concept even further than what you can from Skoog.

To attest as how good this book is: Skoog's book was our main textbook while Harris was our supplement textbook. Towards the middle of the course, with overwhelming demand (and votes) from the students- Harris became the primary textbook taught through the rest of the Analytical Chemistry course. That's how wonderful this book is. I don't know what else to say but that you will learn alot from this book, perhaps more than any other textbooks out there.
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3 of 3 people found the following review helpful By student09 on December 22, 2010
Format: Hardcover Verified Purchase
Although big and heavy, this text is well-written. Plain, clear, and simple to understand. It also provides an excellent review of general and physical chemistry.
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4 of 5 people found the following review helpful By mborobia on August 21, 2012
Format: Hardcover
Great customer service and quick delivery. I bought the textbook for my Analytical Chemistry course. I arrived very promptly and in great condition... just in time for my first chem test. I was worried about whether the international edition had different content and problems... it's an exact copy of the American edition, and less than half the price!
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4 of 5 people found the following review helpful By hector arias on January 14, 2013
Format: Loose Leaf Verified Purchase
I liked saving money on the loose leaf version and it was easy to put it a binder. The paper was thin though and looks like the holes will rip easily (though you use hole protectors as needed which is what I plan to do).
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1 of 1 people found the following review helpful By Scott Whitman on December 28, 2013
Format: Hardcover Verified Purchase
Arguably one of the best textbooks I have ever used. Harris is simultaneously clear and succinct, both often rare qualities in a textbook. Moreover, he draws on a style of writing unusually casual for such a textbook, which in the mind of a student used to dull and even monotonic readings sets this one apart. At times Harris successfully ventures into the realm of humor, even as he still effectively conveys the given material (unicorns for instance were one of many topics I never expected to see mentioned in the context of chemistry). Clear, no-nonsense descriptions, explanations, and diagrams meanwhile convey the topics of each chapter effectively, while the above writing style keeps a student such as myself actively involved in the reading. The end result is the most engaging textbook I have seen to date, and which should be held aloft as a shining example of how to compose an instructive piece on most any topic.
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3 of 4 people found the following review helpful By The Alchemist on September 10, 2012
Format: Hardcover
Harris' Quantitative Chemical Analysis is a wonderful, comprehensive text on quantitative chemical analysis. Daniel Harris is an author who makes analytical chemistry come to life for students by coupling his almost cheeky writing style with numerous real-world examples of analytical chemistry applications. The text has explanations of even complex topics given with the ease like you'd get from your favorite professor's lectures. It has a rather thorough treatment of electrochemistry and spectrophotometry, including fair amounts of background information in addition to their analyical uses. Mass spectrometry is touched on decently--complete with simple explanations about the different types of mass spectrometers in use and how to interpret some mass spectra. There are four chapters dedicated to chromatography, complete with an introduction to separations, GC, LC, and CE. Whether you'll be using this as textbook for a class, an easy-to-use reference, or just for reading on your own, Quantitative Chemical Analysis by Harris is an excellent book.
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