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Solid Phase Microextraction: Theory and Practice [Hardcover]

Janusz Pawliszyn (Author)
5.0 out of 5 stars  See all reviews (1 customer review)

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Book Description

April 21, 1997 0471190349 978-0471190349 1
Solid Phase Microextraction: Theory and Practice Janusz Pawliszyn Solid phase microextraction (SPME) is a recently proposed solvent-free sampling and sample preparation technique. SPME represents a quick, sensitive, and economical approach that can be adopted for field work and can be easily integrated with present analytical instrumentation into an automation process. Written by the inventor of the technique, Solid Phase Microextraction: Theory and Practice describes the theoretical and practical aspects of this new technology, which received an "R&D 100" Award in 1994 recognizing its invention as a major advancement in the analytical sciences. Solid Phase Microextraction: Theory and Practice, the first book on SPME, offers the reader:
* An overview of SPME technique, theory, method development, and applications;
* Experiments for beginners;
* A summary of the practical applications of SPME in environmental, food, pharmaceutical, and forensic settings;
* Material suitable for SPME courses or self-guided study.

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From the Back Cover

Solid Phase Microextraction: Theory and Practice Janusz Pawliszyn Solid phase microextraction (SPME) is a recently proposed solvent-free sampling and sample preparation technique. SPME represents a quick, sensitive, and economical approach that can be adopted for field work and can be easily integrated with present analytical instrumentation into an automation process. Written by the inventor of the technique, Solid Phase Microextraction: Theory and Practice describes the theoretical and practical aspects of this new technology, which received an "R&D 100" Award in 1994 recognizing its invention as a major advancement in the analytical sciences. Solid Phase Microextraction: Theory and Practice, the first book on SPME, offers the reader:
* An overview of SPME technique, theory, method development, and applications;
* Experiments for beginners;
* A summary of the practical applications of SPME in environmental, food, pharmaceutical, and forensic settings;
* Material suitable for SPME courses or self-guided study.

About the Author

Janusz Pawliszyn is Professor of Chemistry at the University of Waterloo, Ontario, Canada. The primary focus of his research program is the design of highly automated and integrated instrumentation for the isolation of organic materials from complex matrices and the subsequent separation, identification, and determination of these species. For his pioneering work, Professor Pawliszyn received the 1995 McBryde Medal, the 1996 Tswett Medal, the 1996 Hyphenated Techniques in Chromatography Award, and the 1996 Caledon Award. He is a member of the Editorial Boards of the Journal of Microcolumn Separations. The Analyst, and Field Analytical Chemistry and Technology. He presently holds the Supelco-Varian-NSERC Industrial Research Chair in New Analytical Methods and Technologies.

Product Details

  • Hardcover: 264 pages
  • Publisher: Wiley-VCH; 1 edition (April 21, 1997)
  • Language: English
  • ISBN-10: 0471190349
  • ISBN-13: 978-0471190349
  • Product Dimensions: 9.5 x 6.3 x 0.7 inches
  • Shipping Weight: 1.1 pounds (View shipping rates and policies)
  • Average Customer Review: 5.0 out of 5 stars  See all reviews (1 customer review)
  • Amazon Best Sellers Rank: #1,691,465 in Books (See Top 100 in Books)

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6 of 6 people found the following review helpful:
5.0 out of 5 stars The first book you have to read about SPME!, May 12, 2000
By A Customer
This review is from: Solid Phase Microextraction: Theory and Practice (Hardcover)
This book was written by Prof Janusz Pawliszyn of Waterloo University (Toronto, Canada), the maker of SPME, a new solvent-free technique which combine sample preparation and sampling, and is a milestone for new millennium chemistry. Theoretical basis of SPME (thermodynamics and kinetics) are well explained and the steps for the development of method are thoroughly described. The book is complete with application notes about sampling in different matrixes and examples of use of this powerful technique in different fields (clinical, forensic, pharmaceutical), and take a look at future applications (e.g. industrial hygiene, field and biological samples, in-fibre derivatization). A very good book essential for chemists and not only for chemists....strongly recommended!
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Inside This Book (learn more)
First Sentence:
The analytical procedure has several steps: sampling, sample preparation, separation, quantitation, statistical evaluation, and decision (see Figure 1.1). Read the first page
Key Phrases - Statistically Improbable Phrases (SIPs): (learn more)
standard methanolic solution, static aqueous phase, equilibration time profiles, withdraw the fiber, extraction time profile, appropriate distribution constants, perfect agitation conditions, native analytes, distribution constant can, phase microextraction, vial equipped, extracting phase, ppb solution, fiber coating, analyte extracted, gaseous headspace, extracted analytes, expose the fiber, caffeine solution, analyte vapor, volatile analytes, fibre coating, coating volume, needle opening, oven temperature program
Key Phrases - Capitalized Phrases (CAPs): (learn more)
Pawliszyn Anal, High Resolut, New York, University of Waterloo, Pawliszyn Environ, Clarendon Press, Food Chem, Source Adopted
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