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Spectrometric Identification of Organic Compounds
 
 

Spectrometric Identification of Organic Compounds [Hardcover]

Robert M. Silverstein (Author), Francis X. Webster (Author)
3.7 out of 5 stars  See all reviews (12 customer reviews)


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Book Description

0471134570 978-0471134572 November 1997 6
This book is characterized by its problem-solving approach with extensive reference charts and tables. First published in 1962, this was the first book on the identification of organic compounds using spectroscopy. Now considered a classic, it can be found on the shelf of every Organic Chemist. The key strength of this text is the extensive set of real-data problems in Chapters 8 and 9. Even professional chemists use these spectra as reference data. Spectrometric Identification of Organic Compounds is written by and for organic chemists, and emphasizes the synergistic effect resulting from the interplay of the spectra.


Product Details

  • Hardcover: 496 pages
  • Publisher: Wiley; 6 edition (November 1997)
  • Language: English
  • ISBN-10: 0471134570
  • ISBN-13: 978-0471134572
  • Product Dimensions: 11.1 x 9 x 1 inches
  • Shipping Weight: 2.9 pounds
  • Average Customer Review: 3.7 out of 5 stars  See all reviews (12 customer reviews)
  • Amazon Best Sellers Rank: #382,149 in Books (See Top 100 in Books)

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Customer Reviews

12 Reviews
5 star:
 (4)
4 star:
 (2)
3 star:
 (5)
2 star:    (0)
1 star:
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Average Customer Review
3.7 out of 5 stars (12 customer reviews)
 
 
 
 
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Most Helpful Customer Reviews

6 of 6 people found the following review helpful:
4.0 out of 5 stars Excellent excercises..., March 12, 2006
It's an OK book if you are a novice in the Spectroscopy determination area, but a very nice book if it's going to be used as a reference book. It's very handy and explains the principles of the Spectroscopic and Spectrometric determinations in a very understandable way. Moreover, the excercises are challenging, making this book and excellent tool for those students interested in learning how to determine structures out of some spectra, although the spectra sometimes are so clean that they don't correspond with the one's that are taken by routine. The weak points of this book are the IR chapter and the lack of a UV chapter explaining various useful techniques for structural determination such as ORD and CD. The NMR section is just OK, but there are more details to be explained in the 2-D NMR NOESY, TOCSY and ROESY. I think the Mass Chapters are the best that any single book has offered to me so far to understand quite easily how powerful is the GCMS as a tool for the Structural Determination of Organic Compounds.
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5 of 5 people found the following review helpful:
3.0 out of 5 stars Great material, regular text..., July 16, 2001
By 
Carlos Valdez (Castro Valley, CA United States) - See all my reviews
This review is from: Spectrometric Identification of Organic Compounds (Hardcover)
The book is subdivided into only 3 of the 4 classical methods for spectrometric identification of compounds: IR, MS, and finally NMR (covering 1H, 13C and very little of 19F and 31P). UV is left out in this edition, so maybe getting a hold of the old edition's UV chapter (which is extremely well-written) might be desired. The MS and the IR chapters are also well-written and explained out. It is in the main technique (NMR) that the author fails to deliver the subject in a straightforward manner and lacks what I think is most important in this field: a large number of exercises and problems.
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7 of 8 people found the following review helpful:
3.0 out of 5 stars Reference vs. Teaching Material, March 4, 2005
This review is from: Spectrometric Identification of Organic Compounds (Hardcover)
This book has wonderful charts and tables for quick referencing, however it is sorely lacking in demonstrations and worked out examples for students new to the subject. The chapters are painfully slow and complex when explaining the theory behind the spectrometric methods and effects on classes of molecules. In short, don't use this book to learn the material unless you already know it. It is a comprehensive reference, but not an effective textbook to teach from.
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Inside This Book (learn more)
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First Sentence:
The concept of mass spectrometry is relatively simple: A compound is ionized (ionization method), the ions are separated on the basis of their mass/charge ratio (ion separation method), and the number of ions representing each mass/charge "unit" is recorded as a spectrum. Read the first page
Key Phrases - Statistically Improbable Phrases (SIPs): (learn more)
ppm cosy, characteristic group absorptions, variable pulse angle, chemical shift equivalence, olefinic methine, difference spectrometry, weak molecular ion peak, ppm correlates, chemical shift equivalent, carbon axis, proton axis, reagent gas methane, caryophyllene oxide, hydrogen deficiency, electrical quadrupole moment, diastereotopic protons, adjacent hydrogen atoms, enantiotopic protons, magnetic equivalence, allylic cleavage, scissoring vibration, hydrocarbon pattern, protons couple, coupled spectrum, acquisition pulse
Key Phrases - Capitalized Phrases (CAPs): (learn more)
New York, Academic Press, Mass Spectrometrv, Plenum Press, Coupling of Protons, Oxford University Press, Sadtler Research Laboratories, Pergamon Press, Stereochemical Anal, Varian Associates, Appendix Chart, Boca Raton, Infrared Band Handbook, John Wiley, Practical Course, Primary Secondary Tertiary, San Francisco, Elsevier Science, Organic Chemistrv, Registry of Mass Spectral Data, Sadder Research Laboratories, University Science Books
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