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Spectrometric identification of organic compounds
  
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Spectrometric identification of organic compounds (Unknown Binding)

by Robert Milton Silverstein (Author) "The concept of mass spectrometry is relatively simple: A compound is ionized (ionization method), the ions are separated on the basis of their mass/charge ratio..." (more)
Key Phrases: ppm cosy, characteristic group absorptions, variable pulse angle, New York, Academic Press, Mass Spectrometrv (more...)
3.7 out of 5 stars See all reviews (7 customer reviews)


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Editorial Reviews

Product Description
This book is characterized by its problem-solving approach with extensive reference charts and tables. First published in 1962, this was the first book on the identification of organic compounds using spectroscopy. Now considered a classic, it can be found on the shelf of every Organic Chemist. The key strength of this text is the extensive set of real-data problems in Chapters 8 and 9. Even professional chemists use these spectra as reference data. Spectrometric Identification of Organic Compounds is written by and for organic chemists, and emphasizes the synergistic effect resulting from the interplay of the spectra. --This text refers to an out of print or unavailable edition of this title.

Product Details

  • Unknown Binding: 256 pages
  • Publisher: Wiley; 2nd edition (1968)
  • Language: English
  • ASIN: B0007EOZH8
  • Average Customer Review: 3.7 out of 5 stars See all reviews (7 customer reviews)
  • Amazon.com Sales Rank: #3,310,144 in Books (See Bestsellers in Books)

Inside This Book (learn more)
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First Sentence:
The concept of mass spectrometry is relatively simple: A compound is ionized (ionization method), the ions are separated on the basis of their mass/charge ratio (ion separation method), and the number of ions representing each mass/charge "unit" is recorded as a spectrum. Read the first page
Key Phrases - Statistically Improbable Phrases (SIPs): (learn more)
ppm cosy, characteristic group absorptions, variable pulse angle, chemical shift equivalence, olefinic methine, difference spectrometry, weak molecular ion peak, ppm correlates, chemical shift equivalent, carbon axis, proton axis, reagent gas methane, caryophyllene oxide, hydrogen deficiency, electrical quadrupole moment, diastereotopic protons, adjacent hydrogen atoms, enantiotopic protons, magnetic equivalence, allylic cleavage, scissoring vibration, hydrocarbon pattern, protons couple, coupled spectrum, acquisition pulse
Key Phrases - Capitalized Phrases (CAPs): (learn more)
New York, Academic Press, Mass Spectrometrv, Plenum Press, Coupling of Protons, Oxford University Press, Sadtler Research Laboratories, Pergamon Press, Stereochemical Anal, Varian Associates, Appendix Chart, Boca Raton, Infrared Band Handbook, John Wiley, Practical Course, Primary Secondary Tertiary, San Francisco, Elsevier Science, Organic Chemistrv, Registry of Mass Spectral Data, Sadder Research Laboratories, University Science Books
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Customer Reviews

7 Reviews
5 star:
 (2)
4 star:
 (1)
3 star:
 (4)
2 star:    (0)
1 star:    (0)
 
 
 
 
 
Average Customer Review
3.7 out of 5 stars (7 customer reviews)
 
 
 
 
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Most Helpful Customer Reviews

 
4 of 4 people found the following review helpful:
4.0 out of 5 stars Excellent excercises..., March 12, 2006
It's an OK book if you are a novice in the Spectroscopy determination area, but a very nice book if it's going to be used as a reference book. It's very handy and explains the principles of the Spectroscopic and Spectrometric determinations in a very understandable way. Moreover, the excercises are challenging, making this book and excellent tool for those students interested in learning how to determine structures out of some spectra, although the spectra sometimes are so clean that they don't correspond with the one's that are taken by routine. The weak points of this book are the IR chapter and the lack of a UV chapter explaining various useful techniques for structural determination such as ORD and CD. The NMR section is just OK, but there are more details to be explained in the 2-D NMR NOESY, TOCSY and ROESY. I think the Mass Chapters are the best that any single book has offered to me so far to understand quite easily how powerful is the GCMS as a tool for the Structural Determination of Organic Compounds.
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4 of 4 people found the following review helpful:
3.0 out of 5 stars Reference vs. Teaching Material, March 4, 2005
This book has wonderful charts and tables for quick referencing, however it is sorely lacking in demonstrations and worked out examples for students new to the subject. The chapters are painfully slow and complex when explaining the theory behind the spectrometric methods and effects on classes of molecules. In short, don't use this book to learn the material unless you already know it. It is a comprehensive reference, but not an effective textbook to teach from.
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4 of 4 people found the following review helpful:
3.0 out of 5 stars Great material, regular text..., July 16, 2001
By Carlos Valdez (Castro Valley, CA United States) - See all my reviews
The book is subdivided into only 3 of the 4 classical methods for spectrometric identification of compounds: IR, MS, and finally NMR (covering 1H, 13C and very little of 19F and 31P). UV is left out in this edition, so maybe getting a hold of the old edition's UV chapter (which is extremely well-written) might be desired. The MS and the IR chapters are also well-written and explained out. It is in the main technique (NMR) that the author fails to deliver the subject in a straightforward manner and lacks what I think is most important in this field: a large number of exercises and problems.
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Most Recent Customer Reviews

3.0 out of 5 stars a good book with a series useful data bases
it is our required textbook for organospectroscopy course. it provides a series of useful databases, which is good for future resaerch. Read more
Published 17 months ago by Li Jing

5.0 out of 5 stars Sixth edition is what is available now and is excellent.
Wiley says this seventh edition is due out October 2004.
Published on November 19, 2003

5.0 out of 5 stars An Important book
This book provide a the basis of the fundamentals of Spectroscopy in many fields (IR, HNMR, CNMR, DEPT, COSY, HMBC, HMQC, TOCSY, MS, and much more) It has many real problems in an... Read more
Published on May 10, 2000 by Christian Romero

3.0 out of 5 stars Good in NMR Spectra analysis information, but weak elsewhere
This book lacked information in my opinion. Silverstein started a good project but just didn't give enough information about IR interpretation, mass spec, C-13 NMR, etc. Read more
Published on November 19, 1999 by Clarke B Taylor

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