Static Headspace-Gas Chromatography Theory and Practice Bruno Kolb * Leslie S. Ettre Static (equilibrium) headspace-gas chromatography (static HS-GC) offers a reliable, simple, and accurate way to quantitate volatile compounds in liquid and solid matrices. The technique is being used in increasingly more analytical laboratories in a variety of industries because it enables high sample turnaround, automated high-performance GC analysis, and automated and unattended sample clean-up by gas extraction, while avoiding laborious sample preparation. Static Headspace-Gas Chromatography provides the most thorough and current treatment available on this technique. The book covers the theory of headspace sampling as related to selection of the operational parameters, describes quantitative calibration techniques, and presents, and presents detailed methods, all adapted for automation. It includes many examples of proven practical applications-complete with original data-from the most important applications of static HS-GC in environmental analysis, polymers, packaging, pharmaceuticals, and food analysis.
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Book Description
Editorial Reviews
Review
"This is an important resource on an increasingly useful technique. It should be in the library of any chromatographer...Essential." (CHOICE, November 2006)
From the Publisher
This text emphasizes the techniques, methods and procedures of static headspace-gas chromatography (HS-GC). It covers the theory of headspace sampling as related to selection of the operational parameters, describes quantitative calibration techniques, and presents detailed methods, all adapted for automation. It includes many examples of proven practical applications--complete with original data--from the most important applications of static HS-GC in environmental analysis, polymers, packaging, pharmaceuticals, and food analysis.
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Most Helpful Customer Reviews
3 of 3 people found the following review helpful:
4.0 out of 5 stars
Great static headspace reference book,
By
This review is from: Static Headspace—Gas Chromatography: Theory and Practice (Hardcover)
Substantially revised, this book is definitely a must have for chromatographers who practice static (and even dynamic) headspace technique. All key aspects and factors influencing headspace were thoroughly discussed. Strategies in gaining sensitivity and selectivity were proposed - heat, mechanical shaking, sonication, addition of various salts to name a few. All in all, a great book to keep for reference
5.0 out of 5 stars
Good choice!,
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This review is from: Static Headspace-Gas Chromatography: Theory and Practice (Hardcover)
If you need be an expert in HS-GC buy it! It's a very detailed book.
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Inside This Book
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First Sentence:
Gas chromatography is an analytical technique for the investigation of volatile compounds. Read the first page Key Phrases - Statistically Improbable Phrases (SIPs): (learn more)
thermostatting time, headspace sensitivity, sample transfer time, liquid displacer, thermostatting temperature, balanced pressure system, methyl silicone stationary phase, cryogenic sample concentration, phase ratio values, full evaporation technique, continuous gas extraction, electrolytic plating bath, peak area values, hexyl cellosolve, volatile sample components, obtained peak area, multiple headspace extraction, headspace vial, splitless sampling, vapor standard, pressurization time, bonded phenyl, minutes isothermal, laminated plastic film, vial pressure Key Phrases - Capitalized Phrases (CAPs): (learn more)
New York, Gas Chromatographic Headspace Analysis, Perkin-Elmer Corporation, Mikrochim Acta, Pharmacopeial Forum, Use of External Standard, Compound Concentration, Examination of Water New!
Books on Related Topics | Concordance | Text Stats Browse Sample Pages:
Front Cover | Table of Contents | First Pages | Index | Back Cover | Surprise Me!
Gas chromatography is an analytical technique for the investigation of volatile compounds. Read the first page Key Phrases - Statistically Improbable Phrases (SIPs): (learn more)
thermostatting time, headspace sensitivity, sample transfer time, liquid displacer, thermostatting temperature, balanced pressure system, methyl silicone stationary phase, cryogenic sample concentration, phase ratio values, full evaporation technique, continuous gas extraction, electrolytic plating bath, peak area values, hexyl cellosolve, volatile sample components, obtained peak area, multiple headspace extraction, headspace vial, splitless sampling, vapor standard, pressurization time, bonded phenyl, minutes isothermal, laminated plastic film, vial pressure Key Phrases - Capitalized Phrases (CAPs): (learn more)
New York, Gas Chromatographic Headspace Analysis, Perkin-Elmer Corporation, Mikrochim Acta, Pharmacopeial Forum, Use of External Standard, Compound Concentration, Examination of Water New!
Books on Related Topics | Concordance | Text Stats Browse Sample Pages:
Front Cover | Table of Contents | First Pages | Index | Back Cover | Surprise Me!
Citations (learn more)
This book cites 13
books:
See all 13 books this book cites
5
books
cite this book:
- Applied Headspace Gas Chromatography by B. Kolb on 5 pages
- Gas Chromatographic Headspace Analysis by H. Hachenberg on 4 pages
- Handbook of Chemistry and Physics, 68th Edition by Robert C. Weast on page 43, and page 285
- Basic Relationships of Gas Chromatography by Leslie S. Ettre on page 8, and page 286
- Analysis of Food Contaminants by John Gilbert on page 10, and page 210
See all 13 books this book cites
- Trace Environmental Quantitative Analysis: Principles: Techniques, and Applications by Paul R. Loconto on page 250
- Methods for Environmental Trace Analysis (Analytical Techniques in the Sciences (AnTs) *) by John R. Dean on page 222
- Sample Preparation Techniques in Analytical Chemistry by Somenath Mitra on page 224
- Chromatography: Concepts and Contrasts by James M. Miller on page 421
- Static Headspace-Gas Chromatography: Theory and Practice by Bruno Kolb in Front Matter
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