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Supercritical Fluid Extraction
 
 
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Supercritical Fluid Extraction [Hardcover]

Larry T. Taylor (Author)

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Book Description

February 28, 1996 0471119903 978-0471119906 1
Clear, Practical Coverage of an Important Reemerging Technology Supercritical Fluid Extraction provides a clear, practical, step-by-step introduction to a sample preparation method that helps laboratories reduce or eliminate the use of halogenated solvents, extract samples more quickly and efficiently, and improve the accuracy of their results. By encouraging a deliberate, systematic approach to supercritical fluid extraction (SFE) methods and techniques, this book enables scientists and technicians to avoid disappointing results and erroneous conclusions and develop reliable guidelines for using this versatile technology. It demonstrates how to make the most of a process that is highly reproducible, fast, and quantitative at sub-ppb levels; preserves the chemical integrity of the analyte to be extracted; and yields a concentrated sample solution that can be easily manipulated. Topics covered include:
* Properties of supercritical fluids
* Functional group solubility in supercritical fluids
* Collection efficiency in off-line SFE
* Extraction strategies
* Applications of analytical SFE
For analytical chemists, technicians, and laboratory managers, this book is the key to a technology that can make every sample extraction and analysis cleaner, more efficient, and more reliable.

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Editorial Reviews

From the Publisher

Using a practical approach, this timely book enables readers with no exposure to this technique to gain a proficient working knowledge of the principles underlying this sample preparation method along with general operating guidelines for its execution including system parameters such as fluid, density, pressure, temperature, flow rate, analyte collection and extraction time.

From the Back Cover

Clear, Practical Coverage of an Important Reemerging Technology Supercritical Fluid Extraction provides a clear, practical, step-by-step introduction to a sample preparation method that helps laboratories reduce or eliminate the use of halogenated solvents, extract samples more quickly and efficiently, and improve the accuracy of their results. By encouraging a deliberate, systematic approach to supercritical fluid extraction (SFE) methods and techniques, this book enables scientists and technicians to avoid disappointing results and erroneous conclusions and develop reliable guidelines for using this versatile technology. It demonstrates how to make the most of a process that is highly reproducible, fast, and quantitative at sub-ppb levels; preserves the chemical integrity of the analyte to be extracted; and yields a concentrated sample solution that can be easily manipulated. Topics covered include:
  • Properties of supercritical fluids
  • Functional group solubility in supercritical fluids
  • Collection efficiency in off-line SFE
  • Extraction strategies
  • Applications of analytical SFE
For analytical chemists, technicians, and laboratory managers, this book is the key to a technology that can make every sample extraction and analysis cleaner, more efficient, and more reliable.

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Inside This Book (learn more)
First Sentence:
The first reported observation of the occurrence of a supercritical phase was made by Baron Cagniard de la Tour in 1822. Read the first page
Key Phrases - Statistically Improbable Phrases (SIPs): (learn more)
versus trap temperature, restrictor plugging, polarity mix, liquid modifier, restrictor tip, collection solvent, solvating strength, fixed restrictor, restrictor temperatures, extraction vessel, naphthalene solubility, variable restrictor, extracted analyte, rinse solvent, sorbent trapping, modified fluids, accumulation device, solvent trap, trap temperatures, dynamic extraction, static extraction, trapping solvent, extraction profile, trap solvent, analyte solubility
Key Phrases - Capitalized Phrases (CAPs): (learn more)
United States, Aceto Naph Tetra, Scott Specialty Gases, Applied Separations, American Chemical Society, Density Considerations, Modifier Introduction, New York, Nile Red, Off-Line Supercritical Fluid Extraction, Suprex Corp, Analyte Recovery, Chemical Abstracts, Symposium Series
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