Previously by Angelici, this laboratory manual for an upper-level undergraduate or graduate course in inorganic synthesis has for many years been the standard in the field. In this newly revised third edition, the manual has been extensively updated to reflect new developments in inorganic chemistry. Twenty-three experiments are divided into five sections: solid state chemistry, main group chemistry, coordination chemistry, organometallic chemistry, and bioinorganic chemistry. The included experiments are safe, have been thoroughly tested to ensure reproducibility, are illustrative of modern issues in inorganic chemistry, and are capable of being performed in one or two laboratory periods of three or four hours. Because facilities vary from school to school, the authors have included a broad range of experiments to help provide a meaningful course in almost any academic setting. Each clearly written & illustrated experiment begins with an introduction that hig! hlights the theme of the experiment, often including a discussion of a particular characterization method that will be used, followed by the experimental procedure, a set of problems, a listing of suggested Independent Studies, and literature references.
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This is an excellent update to a classic inorganic chemistry laboratory text. --Professor Margret J. Geselbracht, Reed College
It is highly recommended as a textbook for a one-semester advanced inorganic synthesis course. --Synth. React. Inorg. Met. Org.
It is highly recommended as a textbook for a one-semester advanced inorganic synthesis course. --Synth. React. Inorg. Met. Org.
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The authors are both professors in the chemistry department of the University of Illinois, Urbana.
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This review is from: Synthesis and Technique in Inorganic Chemistry: A Laboratory Manual (Paperback)
A course on inorganic synthesis and reactions should involve the preparation of inorganic compounds using vacuum line, air- and moisture-exclusion, electrochemical, high-pressure and other synthetic techniques. It should investigate the kinetic and mechanistic studies of inorganic compounds."Synthesis and Techniques in Inorganic Chemistry" simply fulfills all the above purposes. While undergraduate chemistry usually doesn't focus on inorganic laboratory, text written with this much details is a rarity. With 23 experiments and an appendix on techniques, this lab text covers cutting-edge research type of experiments on superconductivity, molecular sieve zeolite-X and buckminsterfullerene (C60). Organometallics is also covered with experiments on organoiron and metal carbonyl cluster. The classical coordination compounds synthesis and mechanism and vacuum line synthesis can also be found in this text. Students can pace and select experiments from all major topic areas over the course of one semester. This is a great resource and reference for modifying existing experiments and shaping up lab techniques.
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First Sentence:
This book is designed to be an introduced to modern research techniques in inorganic chemistry. Read the first page Key Phrases - Statistically Improbable Phrases (SIPs): (learn more)
suction filtration apparatus, greased glass stopper, metal dithiolenes, mulling agent, double manifold, efficient hood, carbonyl ligands, consult your instructor, stirring hot plate, laboratory period, good stopping point, reaction flask, heating mantle, inorganic synthesis, oxidizing equivalents, addition funnel, suction filter, aluminum isopropoxide, dropping funnel, stir bar, vacuum line, lab period, reflux condenser, electron count, distillation flask Key Phrases - Capitalized Phrases (CAPs): (learn more)
New York, Oxford University, Solid State Chemistry, Amino Acid Complexes, American Chemical Society, The Manipulation, Bioinorganic Chemistry, Comprehensive Coordination Chemistry, Englewood Cliffs, The Layered Solids, Courtesy of Kimble, Dalton Trans, Kontes Glass Inc, Organometallic Syntheses, Advanced Inorganic Chemistry, Isotope Natural Abundance, Marcel Dekker, Microscale Synthesis of Vaska's Complex, Mill Valley, Structural Inorganic Chemistry New!
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Front Cover | Table of Contents | First Pages | Index | Back Cover | Surprise Me!
This book is designed to be an introduced to modern research techniques in inorganic chemistry. Read the first page Key Phrases - Statistically Improbable Phrases (SIPs): (learn more)
suction filtration apparatus, greased glass stopper, metal dithiolenes, mulling agent, double manifold, efficient hood, carbonyl ligands, consult your instructor, stirring hot plate, laboratory period, good stopping point, reaction flask, heating mantle, inorganic synthesis, oxidizing equivalents, addition funnel, suction filter, aluminum isopropoxide, dropping funnel, stir bar, vacuum line, lab period, reflux condenser, electron count, distillation flask Key Phrases - Capitalized Phrases (CAPs): (learn more)
New York, Oxford University, Solid State Chemistry, Amino Acid Complexes, American Chemical Society, The Manipulation, Bioinorganic Chemistry, Comprehensive Coordination Chemistry, Englewood Cliffs, The Layered Solids, Courtesy of Kimble, Dalton Trans, Kontes Glass Inc, Organometallic Syntheses, Advanced Inorganic Chemistry, Isotope Natural Abundance, Marcel Dekker, Microscale Synthesis of Vaska's Complex, Mill Valley, Structural Inorganic Chemistry New!
Books on Related Topics | Concordance | Text Stats Browse Sample Pages:
Front Cover | Table of Contents | First Pages | Index | Back Cover | Surprise Me!
Citations (learn more)
This book cites 90
books:
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- Organometallic Syntheses: v. 1 by R.B. King on 4 pages
- The Manipulation of Air-Sensitive Compounds, 2nd Edition by Duward F. Shriver on 4 pages
- Inorganic Chemistry, Third Edition w/CD by Duward Shriver on page 73, page 188, and page 195
- advanced practical inorganic and metalorganic chemistry by R. John Errington on page 12, page 73, and page 180
- Structural Inorganic Chemistry by A. F. Wells on page 13, page 26, and page 35
See all 90 books this book cites
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