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Synthesis and Technique in Inorganic Chemistry: A Laboratory Manual

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A course on inorganic synthesis and reactions should involve the preparation of inorganic compounds using vacuum line, air- and moisture-exclusion, electrochemical, high-pressure and other synthetic techniques. It should investigate the kinetic and mechanistic studies of inorganic compounds.

"Synthesis and Techniques in Inorganic Chemistry" simply fulfills all the above purposes. While undergraduate chemistry usually doesn't focus on inorganic laboratory, text written with this much details is a rarity.

With 23 experiments and an appendix on techniques, this lab text covers cutting-edge research type of experiments on superconductivity, molecular sieve zeolite-X and buckminsterfullerene (C60). Organometallics is also covered with experiments on organoiron and metal carbonyl cluster. The classical coordination compounds synthesis and mechanism and vacuum line synthesis can also be found in this text.

Students can pace and select experiments from all major topic areas over the course of one semester. This is a great resource and reference for modifying existing experiments and shaping up lab techniques.