Organic Solvents Physical Properties and Methods of Purification, Fourth Edition (Volume II in the Techniques of Chemistry series, Edited by Arnold Weissberger) Edited by John A. Riddick, William B. Bunger, and Theodore K. Sakano This fourth edition updates and expands the material of the 15-year-old third edition. Besides revising the physical properties of preparation techniques for previously noted solvents, over 150 new solvents nave been added, many selected to complete groups of isomers and expand homologous series listed in the previous edition. Several isomeric and homologous series are initiated here, including the xylenols, chlorinated toluenes, xylidenes, picolines, lutidines, and silanes. 1986 (0 471-08467-0) 1,325 pp. Physical Methods of Chemistry Volume One: Components of Scientific Instruments and Applications of Computers to Chemical Research, Second Edition Edited by Bryant W. Rossiter and John F. Hamilton Now in a revised Second Edition, the classic Physical Methods of Chemistry series is an independent 8-volume set which surveys the most prevalent methods of determining a wide variety of physical properties of matter. Volume One presents general laboratory techniques common to many of the specific physical methods that are detailed in subsequent volumes. An excellent new work that also serves as a resource of information on a spectrum of components, tools, and techniques that are often used but rarely treated comprehensively in one book. 1986 (0 471-08034-9) 834 pp. Volume Two: Electrochemical Methods, Second Edition Edited by Bryant W. Rossiter and John F. Hamilton Volume Two presents a thorough, up-to-date survey of the applications of electrometric methods in chemical systems. Following an introductory chapter on electrochemical theory common to all electroanalytical methods, it provides information on the latest techniques, especially those with broad applications, including polarography. 1986 (0 471-08027-6) 904 pp.
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The standard reference to theoretical and experimental results on crystal growth. Describes the theories of nucleation and growth in sufficient detail to unify the Experimental sections. Documents the importance of phase relationships, and covers methods of establishing phase diagrams, including directional crystallization, and there is a broad selection of illustrative hot-stage photomicrographs. Reviews laboratory methods of crystallization, both for single-crystal growth and for purification, covering the construction of mechanisms for heating, cooling, stirring, and transport. Provides discussion of the applicability of each method, with respect to sample size and temperature range.
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The simplicity and power of melt crystallization seem to have been overshadowed in recent years by dramatic advances in chromatography. Nevertheless, crystallization remains a simple, effective and economical technique for separation, purification, and growth of single crystals of a wide range of organic and inorganic materials. Quantities ranging from milligrams to kilograms can be processed in the laboratory, economically and in an environmentally desirable way. Techniques of Melt Crystallization summarizes recent progress and provides a contemporary account of melt crystallization techniques useful in the chemical laboratory; it also touches on modern industrial applications. Techniques of Melt Crystallization combines basic theoretical principles of single-stage and multiple-stage crystallization techniques with detailed, up-to-date coverage of a variety of techniques that are not widely practiced and that are within the capabilities of most experimentalists. Laboratory methods for purification, impurity enrichment and growth of single crystals are reviewed. The text covers a wide range of practical details and crystallization modes with useful information on phase diagrams, construction of laboratory equipment, determination of distribution coefficients, and determination of purity Apparatus is described in a "modular" way so that experimenters can select and assemble the most appropriate heating-cooling and transport methods for a particular application. An appendix provides sources of additional information on instrumentation and materials. Computer-generated solutions to the zone-melting equations are presented over a wide range of conditions. This volume will be a valuable and practical reference guide for chemists, physicists, materials scientists and engineers involved in separation, purification and single-crystal growth techniques.
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